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Faint concentric X-ray diffraction rings on a dark detector field

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Residual Stress Determination by X-Ray Diffraction

Measurement runs to ASTM E2860. Welds, machined surfaces and shot-peened parts are read without cutting them, so a specified compressive layer can be verified rather than assumed, and a suspected residual-stress driver confirmed during investigation.


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Overview

Residual-stress measurement by X-ray diffraction quantifies surface and near-surface residual stress in welds, machined components, and shot-peened or surface-treated parts. The sin-squared-psi technique resolves the tensile and compressive stress fields that drive fatigue initiation and stress-corrosion susceptibility, which makes it a primary tool for weld qualification, peening verification, and failure investigation where residual stress is the suspected driver.

What the measurement is

Residual-stress measurement by X-ray diffraction quantifies surface and near-surface residual stress in welds, machined components, and shot-peened or surface-treated parts. The reading is taken without cutting the part, so a specified compressive layer can be verified rather than assumed.

The sin-squared-psi technique resolves the tensile and compressive stress fields locked into a component after welding, machining, grinding, or peening. Tensile residual stress at a surface adds to the service load and drives fatigue initiation and stress-corrosion susceptibility; a controlled compressive layer, for example from shot peening, does the opposite. The measurement separates the two and puts a number on them.

Where it applies

The method is a primary tool for weld qualification, peening verification, and failure investigation where residual stress is the suspected driver.

On a weld, it confirms whether the residual-stress state left by the procedure is acceptable. On a shot-peened or surface-treated part, it verifies that the intended compressive layer is present and of the expected magnitude. In a failure investigation, it confirms or rules out residual stress as a contributor to fatigue or stress-corrosion cracking.

Governing standard

Measurement runs to ASTM E2860, the standard method for residual-stress measurement by X-ray diffraction.

MethodApplicationStandard
Residual-stress measurement by X-ray diffraction (sin-squared-psi)Surface and near-surface residual stress in welds, machined surfaces, and shot-peened or surface-treated partsASTM E2860

The instrument

Measurement is made on an X-ray diffraction spectrometer.

X-ray diffraction analysis investigates the crystalline structure of a material, including atomic arrangement, crystallite size, and imperfections. The X-rays are generated by a cathode ray tube, filtered to produce monochromatic radiation, collimated to concentrate the beam, and directed toward the sample. Residual-stress determination reads the response with specimen tilt to resolve the stress in the surface layer, and the same determination sits inside the NADCAP AC7101 verification scope for aerospace process-verification work. TCR Engineering is a NABL ISO/IEC 17025:2017 accredited laboratory, certificate NABLT0726MH18640.

Related insights

6 of the 135 published insights tagged to Materials Testing bear directly on Residual Stress (XRD). The 6 most relevant are below.

Materials Testing · 2025-05-19

Residual Stress Measurement by XRD

TCR launches Residual Stress Measurement by XRD as per ASTM E2860-20—precision-driven, non-destructive, and standards-compliant.

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Frequently asked questions

Which standard governs residual-stress measurement by X-ray diffraction at TCR?

Measurement runs to ASTM E2860, the standard method for residual-stress measurement by X-ray diffraction. The reading is non-destructive and uses the sin-squared-psi technique. TCR Engineering is a NABL ISO/IEC 17025:2017 accredited laboratory, certificate NABLT0726MH18640.

What components can be measured?

Welds, machined surfaces, and shot-peened or surface-treated parts are read without cutting them, so a specified compressive layer can be verified rather than assumed.

Why is residual stress measured?

Tensile and compressive residual-stress fields drive fatigue initiation and stress-corrosion susceptibility. The measurement supports weld qualification, peening verification, and failure investigation where residual stress is the suspected driver.

Is the method destructive?

No. X-ray diffraction reads the surface and near-surface layer non-destructively, so the part is not sectioned. This makes it suitable for verifying that a specified compressive layer is present.

Measure the residual stress you cannot see.

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